4,7-Bis(dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine

4,7-Bis(dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine Full article

Journal

Molbank
ISSN: 1422-8599

Output data

Year: 2021, Volume: 2021, Number: 4, Article number : M1291, Pages count : DOI: 10.3390/m1291

Authors

Chmovzh Timofey N. ^1,2 , Kudryashev Timofey A. ¹ , Rakitin Oleg A. ¹

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, 47 Leninsky Prospekt, 119991 Moscow, Russia
2	Nanotechnology Education and Research Center, South Ural State University, 76 Lenina Avenue, 454080 Chelyabinsk, Russia

Bis(alkylsulfanyl) derivatives of 1,2,5-thiadiazoles fused with aromatic and heteroaromatic rings containing long alkyl chains are of interest as compounds with liquid crystalline properties. In this communication, 4,7-bis(dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine 1 was obtained from 4,7-dibromo-[1,2,5]thiadiazolo[3,4-c]pyridine 2 by a combination of two reactions—aromatic nucleophilic substitution SNAr and Buchwald–Hartwig cross-coupling. The structure of the newly synthesized compounds was established by means of elemental analysis; high-resolution mass spectrometry; 1H, 13C NMR, IR and UV spectroscopy; and mass spectrometry.

Chmovzh T.N. , Kudryashev T.A. , Rakitin O.A.
4,7-Bis(dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine
Molbank. 2021. V.2021. N4. M1291 . DOI: 10.3390/m1291 WOS Scopus OpenAlex

Web of science:	WOS:000735575000001
Scopus:	2-s2.0-85117892604
OpenAlex:	W3210013260

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OpenAlex	2
Scopus	2
Web of science	2