Synthesis of 4,4'-Bis[3-(Fluorodinitromethyl)-1H-1,2,4-triazol-5-Yl]azofurazan

Synthesis of 4,4'-Bis[3-(Fluorodinitromethyl)-1H-1,2,4-triazol-5-Yl]azofurazan Full article

Journal

Chemistry of Heterocyclic Compounds
ISSN: 1573-8353 , E-ISSN: 0009-3122

Output data

Year: 2020, Volume: 56, Number: 5, Pages: 619-622 Pages count : 4 DOI: 10.1007/s10593-020-02709-1

Authors

Aleksandrova Nataly S. ¹ , Monogarov Konstantin A. ² , Sheremetev Aleksei B. ¹

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russia
2	N. N. Semenov Federal Research Center of Chemical Physics, Russian Academy of Sciences, Moscow, Russia

A three-step method was developed for converting both ethoxycarbonylmethyl groups of 4,4'-bis[3-(ethoxycarbonylmethyl)-1Н-1,2,4-triazol-5-yl]azofurazan into fluorodinitromethyl groups, enabling the preparation of the target 4,4'-bis[3-(fluorodinitromethyl)-1Н-1,2,4-triazol-5-yl]azofurazan in 74% overall yield.

Aleksandrova N.S. , Monogarov K.A. , Sheremetev A.B.
Synthesis of 4,4'-Bis[3-(Fluorodinitromethyl)-1H-1,2,4-triazol-5-Yl]azofurazan
Chemistry of Heterocyclic Compounds. 2020. V.56. N5. P.619-622. DOI: 10.1007/s10593-020-02709-1 WOS Scopus OpenAlex

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