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3,4-Diaminopyridine-2,5-dicarbonitrile Full article

Journal Molbank
ISSN: 1422-8599
Output data Year: 2022, Volume: 2022, Number: 2, Article number : M1386, Pages count : DOI: 10.3390/m1386
Authors Chmovzh Timofey N. 1,2 , Rakitin Oleg A. 1
Affiliations
1 N. D. Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, 47 Leninsky Prospekt, 119991 Moscow, Russia
2 Nanotechnology Education and Research Center, South Ural State University, 76 Lenina Avenue, 454080 Chelyabinsk, Russia

Abstract: Pyridines fused with heterocyclic rings are of great interest as both photovoltaic materials and biologically active compounds. The most convenient precursors for these compounds are pyridine-2,3-diamines. In this communication, 3,4-diaminopyridine-2,5-dicarbonitrile was synthesized by the reaction of 2,5-dibromo-3,4-diaminopyridine with copper cyanide; the best yield of the target compound was achieved by heating the reaction mixture in N,N-dimethylformamide at 120 °C for 6 h. The structure of the newly synthesized compound was established by means of elemental analysis, high resolution mass-spectrometry, 1H, 13C NMR, IR, UV spectroscopy and mass-spectrometry.
Cite: Chmovzh T.N. , Rakitin O.A.
3,4-Diaminopyridine-2,5-dicarbonitrile
Molbank. 2022. V.2022. N2. M1386 . DOI: 10.3390/m1386 WOS Scopus OpenAlex
Identifiers:
Web of science: WOS:000817359200001
Scopus: 2-s2.0-85132556416
OpenAlex: W4283071409
Citing:
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OpenAlex 1
Scopus 1
Web of science 1
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