5,5′-Thiobis(4-chloro-3H-1,2-dithiole-3-thione)

5,5′-Thiobis(4-chloro-3H-1,2-dithiole-3-thione) Full article

Journal

Molbank
ISSN: 1422-8599

Output data

Year: 2022, Volume: 2022, Number: 2, Article number : M1371, Pages count : DOI: 10.3390/m1371

Authors

Ogurtsov Vladimir A. ¹ , Rakitin Oleg A. ¹

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky Prospekt, 119991 Moscow, Russia

3H-1,2-Dithiole-3-thiones are important compounds with many types of significant pharmacological activity. Although many derivatives of this class have been described in the literature, their thioethers have not previously been obtained. In this communication, it is shown that the reaction of 4,5-dichloro-3H-1,2-dithiole-3-thione with potassium isocyanate unexpectedly gave 5,5′-thiobis(4-chloro-3H-1,2-dithiole-3-thione). The structure of the synthesized compound was established by elemental analysis, high-resolution mass spectrometry, 13C NMR and IR spectroscopy, and mass spectrometry.

Ogurtsov V.A. , Rakitin O.A.
5,5′-Thiobis(4-chloro-3H-1,2-dithiole-3-thione)
Molbank. 2022. V.2022. N2. M1371 . DOI: 10.3390/m1371 WOS Scopus OpenAlex

Web of science:	WOS:000817377600001
Scopus:	2-s2.0-85131532994
OpenAlex:	W4281987133

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OpenAlex	1
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