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The formation of tetracyclo[7.2.1.02,5.02,8]dodeca-6,10-dienes under conditions of thermal isomerization of spiro[2.4]hepta-4,6-diene into bicyclo[3.2.0]hepta-1,3-diene Full article

Journal Russian Chemical Bulletin
ISSN: 1573-9171 , E-ISSN: 1066-5285
Output data Year: 1993, Volume: 42, Number: 1, Pages: 118-123 Pages count : 6 DOI: 10.1007/bf00699990
Authors Tomilov Yu.V. 1 , Kostitsyn A.B. 1 , Shulishov E.V. 1 , Nefedov O.M. 1
Affiliations
1 N. D. Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, Moscow, Russian Federation

Abstract: The formation of the novel hydrocarbons, tetracyclo[7.2.1.02,5.02,8]dodecadienes, as a result of thermal isomerization of spiro[2.4]hepta-4,6-diene into bicyclo[3.2.0]hepta-1,3-diene and its capture by 1,3-dienes is demonstrated. The conditions of thermal isomerization and dimerization of the spiroheptadiene are studied. Cyclopropanation of the polycyclic dienes formed by diazomethane in the presence of Pd-catalysts was accomplished, and occured solely through the norbornene double bond.
Cite: Tomilov Y.V. , Kostitsyn A.B. , Shulishov E.V. , Nefedov O.M.
The formation of tetracyclo[7.2.1.02,5.02,8]dodeca-6,10-dienes under conditions of thermal isomerization of spiro[2.4]hepta-4,6-diene into bicyclo[3.2.0]hepta-1,3-diene
Russian Chemical Bulletin. 1993. V.42. N1. P.118-123. DOI: 10.1007/bf00699990 WOS Scopus OpenAlex
Identifiers:
≡ Web of science: WOS:A1993MM95700028
≡ Scopus: 2-s2.0-34249764042
≡ OpenAlex: W2041937374
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