Molecular and Crystal Structures of Bispidine Conjugates and Tempo Radicals | Sciact

Molecular and Crystal Structures of Bispidine Conjugates and Tempo Radicals Научная публикация

Журнал

Journal of Structural Chemistry
ISSN: 1573-8779 , E-ISSN: 0022-4766

Вых. Данные

Год: 2025, Том: 66, Номер: 3, Страницы: 645-652 Страниц : 8 DOI: 10.1134/s0022476625030205

Авторы

Medved′ko A.V. ¹ , Zakirov A.M. ¹ , Minyaev M.E. ¹ , Tretyakov E.V. ¹ , Vatsadze S.Z. ¹

Организации

1	Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russia

Molecular and crystal structures of the following bispidine conjugates with stable TEMPO radicals and their synthetic precursors are described for the first time: 4-(2-bromacetoamido)-2,2,6,6-tetramethylpiperidine-1-oxyl (2), tert-butyl-3,7-diazabicyclo[3.3.1]nonan-3-carboxylate (4), 2-(1-oxyl-2,2,6,6-tetramethylpiperidine-4-yl)acetamide (3,7-diazabicyclo[3.3.1]nonan-3-carboxylate (6) and 2,2′-(1,5-dimethyl-3,7-diazabicyclo[3.3.1]nonan-3,7-diyl)bis[N-(2,2,6,6-tetramethyl-1-oxyl-piperidine-4-yl)acetamide] (7). These conjugates are prepared by the alkylation of bispidines using TEMPO bromo-derivatives.

Medved′ko A.V. , Zakirov A.M. , Minyaev M.E. , Tretyakov E.V. , Vatsadze S.Z.
Molecular and Crystal Structures of Bispidine Conjugates and Tempo Radicals
Journal of Structural Chemistry. 2025. V.66. N3. P.645-652. DOI: 10.1134/s0022476625030205 WOS Scopus OpenAlex

Web of science:	WOS:001456015300017
Scopus:	2-s2.0-105001362386
OpenAlex:	W4408967383

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