New stereoselective synthesis of 5α-androst-1-ene-3β,17β-diol

New stereoselective synthesis of 5α-androst-1-ene-3β,17β-diol Full article

Journal

Russian Chemical Bulletin
ISSN: 1573-9171 , E-ISSN: 1066-5285

Output data

Year: 2023, Volume: 72, Number: 11, Pages: 2726-2730 Pages count : 5 DOI: 10.1007/s11172-023-4078-5

Authors

Chernoburova E.I. ¹ , Shchetinina M.A. ¹ , Korolev V.A. ¹ , Ilovaisky A.I. ¹ , Zavarzin I.V. ¹

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation

Efficient stereoselective methods for the synthesis of 5α-androst-1-ene-3β,17β-diol, which is used as a reference compound for identification of anabolic steroids and their metabolites, were elaborated. The key factor of the synthesis is the use of the sodium borohydride—cerium(III) chloride system as a reducing agent.

Chernoburova E.I. , Shchetinina M.A. , Korolev V.A. , Ilovaisky A.I. , Zavarzin I.V.
New stereoselective synthesis of 5α-androst-1-ene-3β,17β-diol
Russian Chemical Bulletin. 2023. V.72. N11. P.2726-2730. DOI: 10.1007/s11172-023-4078-5 WOS Scopus OpenAlex

Web of science:	WOS:001132088500016
Scopus:	2-s2.0-85180649173
OpenAlex:	W4390416064

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