Selective and efficient electrocatalytic way to spirobarbituric dihydrofurans

Selective and efficient electrocatalytic way to spirobarbituric dihydrofurans Full article

Journal

Mendeleev Communications
ISSN: 1364-551X , E-ISSN: 0959-9436

Output data

Year: 2021, Volume: 31, Number: 3, Pages: 347-349 Pages count : 3 DOI: 10.1016/j.mencom.2021.04.021

Authors

Elinson Michail N. ¹ , Vereshchagin Anatoly N. ¹ , Ryzhkova Yuliya E. ¹ , Egorov Mikhail P. ¹

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 119991 Moscow, Russian Federation

Electrocatalytic cyclization of 6-hydroxy-5-[(2-hydroxy-6-oxocyclohex-1-en-1-yl)(aryl)methyl]-1,3-dimethylpyrimidine-2,4-(1H,3H)-diones in alcohols in an undivided cell in the presence of sodium halides results in selective formation of substituted spirobarbituric dihydrofurans in 82–93% yields. Crystal structure of 3-(3-bromophenyl)-1′,3′,6,6-tetramethyl-3,5,6,7-tetrahydro-2′,4-dihydrospiro[benzofuran-2,5′-pyrimidine]-2′,4,4′,6′(1′H,3′H)-tetraone has been confirmed by X-ray diffraction data.

Elinson M.N. , Vereshchagin A.N. , Ryzhkova Y.E. , Egorov M.P.
Selective and efficient electrocatalytic way to spirobarbituric dihydrofurans
Mendeleev Communications. 2021. V.31. N3. P.347-349. DOI: 10.1016/j.mencom.2021.04.021 Scopus OpenAlex

Scopus:	2-s2.0-85107150933
OpenAlex:	W3172193702

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