Synthesis and structural investigation of 4,4′-dimethyl-[3,3′-bi(1,2,5-oxadiazole)] 5,5′-dioxide

Synthesis and structural investigation of 4,4′-dimethyl-[3,3′-bi(1,2,5-oxadiazole)] 5,5′-dioxide Full article

Journal

Russian Chemical Bulletin
ISSN: 1573-9171 , E-ISSN: 1066-5285

Output data

Year: 2018, Volume: 67, Number: 11, Pages: 2044-2048 Pages count : 5 DOI: 10.1007/s11172-018-2326-x

Authors

Obruchnikova N.V. ¹ , Novikov R.A. ¹ , Zlotin S.G. ¹ , Dorovatovskii P.V. ² , Khrustalev V.N. ^2,3 , Rakitin O.A. ¹

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991, Moscow, Russian Federation
2	National Research Center “Kurchatov Institute”, 1 ul. Akad. Kurchatova, 123182, Moscow, Russian Federation
3	Peoples´ Friendship University of Russia (RUDN University), 6 ul. Miklukho-Maklaya, 117198 Moscow, Russian Federation

The oxidation of hexane-2,3,4,5-tetraone tetraoxime with dinitrogen tetroxide was studied in different solvents. The primary furoxan ring closure was found to occur involving either two central or two terminal oxime groups to form 4,7-dimethyl[1,2,5]oxadiazolo[3,4-d]pyridazine 1,5,6-trioxide and the previously unknown 4,4′-dimethyl-[3,3′-bi(1,2,5-oxadiazole)] 5,5′-dioxide. The structure of the latter compound was established by X-ray diffraction.

Obruchnikova N.V. , Novikov R.A. , Zlotin S.G. , Dorovatovskii P.V. , Khrustalev V.N. , Rakitin O.A.
Synthesis and structural investigation of 4,4′-dimethyl-[3,3′-bi(1,2,5-oxadiazole)] 5,5′-dioxide
Russian Chemical Bulletin. 2018. V.67. N11. P.2044-2048. DOI: 10.1007/s11172-018-2326-x WOS Scopus OpenAlex

Web of science:	WOS:000454510700013
Scopus:	2-s2.0-85059330098
OpenAlex:	W2906788830

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