Step by step and one-pot syntheses of 5-hydroxy-5-(polyfluoroalkyl)isoxazol-4(5H)-one oximes

Step by step and one-pot syntheses of 5-hydroxy-5-(polyfluoroalkyl)isoxazol-4(5H)-one oximes Full article

Journal

Mendeleev Communications
ISSN: 1364-551X , E-ISSN: 0959-9436

Output data

Year: 2018, Volume: 28, Number: 2, Pages: 126-127 Pages count : 2 DOI: 10.1016/j.mencom.2018.03.003

Authors

Palysaeva Nadezhda V. ¹ , Boltacheva Nadezhda S. ² , Slepukhin Pavel A. ² , Pervova Marina G. ² , Filyakova Vera I. ² , Sheremetev Aleksei B. ¹ , Charushin Valery N. ^2,3

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 119991 Moscow, Russian Federation
2	I. Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences, 620990 Ekaterinburg, Russian Federation
3	Institute of Chemical Engineering, Ural Federal University, 620002 Ekaterinburg, Russian Federation

5-Hydroxy-5-(polyfluoroalkyl)isoxazol-4(5H)-one oximes have been obtained by nitrosation of lithium 3-polyfluoroalkyl-1,3-diketonates followed by treatment of intermediate 3-(poly-fluoroalkyl)propane-1,2,3-trione 2-oximes with hydroxylamine hydrochloride. The one-pot protocol comprising both stages has been elaborated.

Palysaeva N.V. , Boltacheva N.S. , Slepukhin P.A. , Pervova M.G. , Filyakova V.I. , Sheremetev A.B. , Charushin V.N.
Step by step and one-pot syntheses of 5-hydroxy-5-(polyfluoroalkyl)isoxazol-4(5H)-one oximes
Mendeleev Communications. 2018. V.28. N2. P.126-127. DOI: 10.1016/j.mencom.2018.03.003 WOS Scopus OpenAlex

≡ Web of science:	WOS:000435626800003
≡ Scopus:	2-s2.0-85044101391
≡ OpenAlex:	W2792189397