Synthesis of condensed pregnano[17,16-d]triazolines under high pressure

Synthesis of condensed pregnano[17,16-d]triazolines under high pressure Full article

Journal

Russian Chemical Bulletin
ISSN: 1573-9171 , E-ISSN: 1066-5285

Output data

Year: 2018, Volume: 67, Number: 2, Pages: 308-312 Pages count : 5 DOI: 10.1007/s11172-018-2075-x

Authors

Sedishev I.P. ¹ , Zharov A.A. ¹ , Levina I.S. ¹ , Tyurin A.Yu. ¹ , Volkova Yu.A. ¹ , Aksenov A.N. ¹ , Kachala V.V. ¹ , Tikhonova T.A. ¹ , Zavarzin I.V. ¹

Affiliations

1	N. D. Zelinsky Institute of the Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation

Condensed pregnano[17,16-d]triazolines were produced in 1,3-dipolar cycloaddition of 16-dehydropregnenolone acetate with organic azides at 10 kbar. The structure of the synthesized compounds was determined by using two-dimensional NMR spectroscopy (1H—1H COSY, NOESY, HSQC, and HMBC).

Sedishev I.P. , Zharov A.A. , Levina I.S. , Tyurin A.Y. , Volkova Y.A. , Aksenov A.N. , Kachala V.V. , Tikhonova T.A. , Zavarzin I.V.
Synthesis of condensed pregnano[17,16-d]triazolines under high pressure
Russian Chemical Bulletin. 2018. V.67. N2. P.308-312. DOI: 10.1007/s11172-018-2075-x WOS Scopus OpenAlex

≡ Web of science:	WOS:000431320200018
≡ Scopus:	2-s2.0-85046656293
≡ OpenAlex:	W2799414403