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Regioselective synthesis of bifuroxanyl systems with the 3-nitrobifuroxanyl core via a one-pot acylation/nitrosation/cyclization cascade Full article

Journal Tetrahedron Letters
ISSN: 0040-4039 , E-ISSN: 1873-3581
Output data Year: 2016, Volume: 57, Number: 38, Pages: 4268-4272 Pages count : 5 DOI: 10.1016/j.tetlet.2016.08.011
Authors Fershtat Leonid L. 1 , Larin Alexander A. 1 , Epishina Margarita A. 1 , Kulikov Alexander S. 1 , Ovchinnikov Igor V. 1 , Ananyev Ivan V. 2 , Makhova Nina N. 1
Affiliations
1 N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47, Leninsky Prosp., 119991 Moscow, Russian Federation
2 A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 Vavilova Str., 119991 Moscow, Russian Federation

Abstract: A regioselective method for the synthesis of previously unknown bifuroxanyl systems containing the 3-nitrobifuroxanyl core, based on a cascade of one-pot reactions comprising of the acylation of dinitromethane sodium salt with furoxanyl hydroxamic acid chlorides, nitrosation of the acylation product with NaNO2/AcOH/AcONa, and intramolecular cyclization of the nitrosation product to give the 3-nitrobifuroxanyl moiety, has been developed.
Cite: Fershtat L.L. , Larin A.A. , Epishina M.A. , Kulikov A.S. , Ovchinnikov I.V. , Ananyev I.V. , Makhova N.N.
Regioselective synthesis of bifuroxanyl systems with the 3-nitrobifuroxanyl core via a one-pot acylation/nitrosation/cyclization cascade
Tetrahedron Letters. 2016. V.57. N38. P.4268-4272. DOI: 10.1016/j.tetlet.2016.08.011 WOS Scopus OpenAlex
Identifiers:
Web of science: WOS:000383313900003
Scopus: 2-s2.0-84984783390
OpenAlex: W2491851015
Citing:
DB Citing
OpenAlex 41
Scopus 45
Web of science 41
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