Preparation of Fe-doped deuterated polyethylene loads for the angara 5-1 high-current generator

Preparation of Fe-doped deuterated polyethylene loads for the angara 5-1 high-current generator Научная публикация

Журнал

Instruments and Experimental Techniques
ISSN: 1608-3180 , E-ISSN: 0020-4412

Вых. Данные

Год: 2015, Том: 58, Номер: 6, Страницы: 817-819 Страниц : 3 DOI: 10.1134/s002044121506010x

Авторы

Pimenov V.G. ¹ , Sheveleva E.E. ¹ , Sakharov A.M. ¹

Организации

1	N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russia

A new method of manufacturing low-density foamed deuterated polyethylene cylinders (20–200 mg/cm3) with a diameter of 1–2 mm and length of 10 mm is designed. Up to 5 wt % Fe dopants can be embedded into the foam for diagnostic analysis. Polyolefine-based microcellular foams are produced by dissolving polymers at high temperatures in aromatic hydrocarbon, subsequently initiating phase separation in a solution (usually during fast cooling) and gel formation. It has been determined that for obtaining high-quality products it is necessary to preliminary cool the system down to 135°C. To avoid wasteful polymer losses, the whole process is carried out in the single ampoule and multiple centrifugation is used for mixing. A solvent is removed using critical-point drying.

Pimenov V.G. , Sheveleva E.E. , Sakharov A.M.
Preparation of Fe-doped deuterated polyethylene loads for the angara 5-1 high-current generator
Instruments and Experimental Techniques. 2015. V.58. N6. P.817-819. DOI: 10.1134/s002044121506010x WOS Scopus OpenAlex

≡ Web of science:	WOS:000365176200019
≡ Scopus:	2-s2.0-84947443832
≡ OpenAlex:	W2292365726