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Extracting 1,3-dimethylpyrazole and 1,5-dimethylpyrazole from binary industrial mixtures Full article

Journal Coke and Chemistry
ISSN: 1068-364X , E-ISSN: 1934-8398
Output data Year: 2015, Volume: 58, Number: 7, Pages: 275-278 Pages count : 4 DOI: 10.3103/s1068364x15070078
Authors Rusak V.V. 1 , Zaretsky M.I. 1 , Semenov V.V. 1 , Chartov E.M. 1 , Ugrak B.I. 1 , Nysenko Z.N. 1
Affiliations
1 Zelinskii Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russia

Abstract: The liquid–vapor phase equilibria in binary systems containing 1,3-dimethylpyrazole and 1,5-dimethylpyrazole are investigated. On the basis of the results, the relative volatility, the minimum and working numbers of theoretical plates, and the minimum and working reflux ratios are calculated, with a view to the production of individual isomers (>99% purity). The results are experimentally confirmed. It proves possible to separate 1,3-dimethylpyrazole and 1,5-dimethylpyrazole by rectification.
Cite: Rusak V.V. , Zaretsky M.I. , Semenov V.V. , Chartov E.M. , Ugrak B.I. , Nysenko Z.N.
Extracting 1,3-dimethylpyrazole and 1,5-dimethylpyrazole from binary industrial mixtures
Coke and Chemistry. 2015. V.58. N7. P.275-278. DOI: 10.3103/s1068364x15070078 WOS Scopus OpenAlex
Identifiers:
Web of science: WOS:000365944700007
Scopus: 2-s2.0-84945200558
OpenAlex: W2275879572
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