A Novel Synthesis of Thioglycolurils by Ring Contraction of 5,7-Dialkyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-ones

A Novel Synthesis of Thioglycolurils by Ring Contraction of 5,7-Dialkyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-ones Full article

Journal

Synthesis-Stuttgart
ISSN: 1437-210X , E-ISSN: 0039-7881

Output data

Year: 2012, Volume: 44, Number: 21, Pages: 3366-3370 Pages count : 5 DOI: 10.1055/s-0032-1317194

Authors

Gazieva Galina ¹ , Poluboyarov Pavel ¹ , Popov Leonid ² , Kolotyrkina Natalya ¹ , Kravchenko Angelina ¹ , Makhova Nina ¹

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
2	Department of Chemistry, Southern Federal University

A new synthetic route to (E)-1,3-dialkyl-4-(benzylideneamino)-5-thioxohexahydroimidazo[4,5-d]imidazol-2(1H)-ones (thioglycolurils), by a ring contraction reaction of 5,7-dialkyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-ones with aromatic aldehydes, has been developed.

Gazieva G. , Poluboyarov P. , Popov L. , Kolotyrkina N. , Kravchenko A. , Makhova N.
A Novel Synthesis of Thioglycolurils by Ring Contraction of 5,7-Dialkyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-ones
Synthesis-Stuttgart. 2012. V.44. N21. P.3366-3370. DOI: 10.1055/s-0032-1317194 WOS Scopus OpenAlex

≡ Web of science:	WOS:000310461400018
≡ Scopus:	2-s2.0-84867896120
≡ OpenAlex:	W2951089975