Synthesis and structures of 5(3H)-oxotetrahydro-1H-imidazo[4,5-c][1,2,5]thiadiazole 2,2-dioxides

Synthesis and structures of 5(3H)-oxotetrahydro-1H-imidazo[4,5-c][1,2,5]thiadiazole 2,2-dioxides Научная публикация

Журнал

Russian Chemical Bulletin
ISSN: 1573-9171 , E-ISSN: 1066-5285

Вых. Данные

Год: 2008, Том: 57, Номер: 8, Страницы: 1744-1753 Страниц : 10 DOI: 10.1007/s11172-008-0231-4

Авторы

Gazieva G.A. ¹ , Kravchenko A.N. ¹ , Lyssenko K.A. ² , Gaziev R.G. ¹ , Lebedev O.V. ¹ , Makhova N.N. ¹

Организации

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991, Moscow, Russian Federation
2	A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 ul. Vavilova, 119991, Moscow, Russian Federation

The reactions of sulfamides with 4,5-dihydroxyimidazolidin-2-ones were studied at ambient and high pressure. The previously unknown derivatives of 5(3H)-oxotetrahydro-1H-imidazo-[4,5-c][1,2,5]thiadiazole 2,2-dioxide, viz., sulfo analogs of tetrahydroimidazo[4,5-d]imidazole-2,5-(1H,3H) diones (glycolurils), were synthesized. The structures of some of these compounds were established by X-ray diffraction. The high-pressure reactions performed under conditions of solvent phase transitions afforded also N-(1,3-diethyl-5-hydroxy-2-oxoimidazolidin-4-yl)-N,N′-dialkylsulfamides. Among these compounds, a new conglomerate was found.

Gazieva G.A. , Kravchenko A.N. , Lyssenko K.A. , Gaziev R.G. , Lebedev O.V. , Makhova N.N.
Synthesis and structures of 5(3H)-oxotetrahydro-1H-imidazo[4,5-c][1,2,5]thiadiazole 2,2-dioxides
Russian Chemical Bulletin. 2008. V.57. N8. P.1744-1753. DOI: 10.1007/s11172-008-0231-4 WOS Scopus OpenAlex

≡ Web of science:	WOS:000268881100025
≡ Scopus:	2-s2.0-68949098495
≡ OpenAlex:	W1976585834