Condensation of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids

Condensation of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids Full article

Journal

Mendeleev Communications
ISSN: 1364-551X , E-ISSN: 0959-9436

Output data

Year: 2010, Volume: 20, Number: 1, Pages: 47-49 Pages count : 3 DOI: 10.1016/j.mencom.2010.01.018

Authors

Vasilevskii Sergei V. ¹ , Belyakov Pavel A. ¹ , Gazieva Galina A. ¹ , Nelyubina Yulia V. ² , Kolotyrkina Natal’ya G. ¹ , Kravchenko Angelina N. ¹

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 119991 Moscow, Russian Federation
2	A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 119991 Moscow, Russian Federation

The reaction of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids was studied, and the directed synthesis of {(5,7-dimethyl-6-oxo-4a,7a-diphenyl-4,4a,5,6,7,7a-hexahydro-1H-imidazo[4,5-e]-1,2,4-triazin-3-yl)thio}acetic acid and 1,3-dimethyl-3a,9a-diphenyl-3,3a,9,9a-tetrahydroimidazo[4,5-e]-1,3-thiazolo[3,2-b]-1,2,4-triazine-2,7(1H,6H)-dione was perfomed for the first time; the structures of title compounds were confirmed by the 1H-{13C} HMBC, 1H-{15N} HSQC, TOCSY, NOESY, HMBC, HSQCED NMR spectroscopy methods and XRD analysis of the tricyclic product.

Vasilevskii S.V. , Belyakov P.A. , Gazieva G.A. , Nelyubina Y.V. , Kolotyrkina N.G. , Kravchenko A.N.
Condensation of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids
Mendeleev Communications. 2010. V.20. N1. P.47-49. DOI: 10.1016/j.mencom.2010.01.018 WOS Scopus OpenAlex

≡ Web of science:	WOS:000274775000018
≡ Scopus:	2-s2.0-74049093046
≡ OpenAlex:	W2950564319