Synthesis of first representatives of 3,3′-bi(6,8-dialkyl-2,4-dioxa-6,8-diazabicyclo[3.3.0]octan-7-ones)

Synthesis of first representatives of 3,3′-bi(6,8-dialkyl-2,4-dioxa-6,8-diazabicyclo[3.3.0]octan-7-ones) Full article

Journal

Journal of Heterocyclic Chemistry
ISSN: 0022-152X , E-ISSN: 1943-5193

Output data

Year: 2006, Volume: 43, Number: 5, Pages: 1295-1302 Pages count : 8 DOI: 10.1002/jhet.5570430523

Authors

Sigachev Andrey S. ¹ , Kravchenko Angelina N. ¹ , Gazieva Galina A. ¹ , Belyakov Pavel A. ¹ , Kolotyrkina Natal'Ya G. ¹ , Lebedev Oleg V. ¹ , Makhova Nina N. ¹ , Lyssenko Konstantin A. ²

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry of Russian Academy of Sciences, 47 Leninsky pr, 119991 Moscow, RUSSIA
2	A. N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, 28 Vavilova str., 119991, Moscow, RUSSIA

The first representatives of 3,3′-bi(2,4-dioxa-6,8-diazabicyclo[3.3.0]octan-7-ones) have been synthesized by a reaction of glyoxal as form of 2,2′-bi(4,5-dihydroxy-1,3-dioxalane) with N,N′-dialkylureas. Their structures have been supported by X-ray analysis. 1,3-Dialkylimidazolidine-2,4-diones (hydantoins) have been isolated as by-products and their formation mechanism has been experimentally confirmed.

Sigachev A.S. , Kravchenko A.N. , Gazieva G.A. , Belyakov P.A. , Kolotyrkina N.G. , Lebedev O.V. , Makhova N.N. , Lyssenko K.A.
Synthesis of first representatives of 3,3′-bi(6,8-dialkyl-2,4-dioxa-6,8-diazabicyclo[3.3.0]octan-7-ones)
Journal of Heterocyclic Chemistry. 2006. V.43. N5. P.1295-1302. DOI: 10.1002/jhet.5570430523 WOS Scopus OpenAlex

≡ Web of science:	WOS:000241541900023
≡ Scopus:	2-s2.0-33750943787
≡ OpenAlex:	W2952485539