Nitropyrazoles. 6. Structure of N-nitropyrazoles and their 13C, 15N, and 14N NMR spectra

Nitropyrazoles. 6. Structure of N-nitropyrazoles and their 13C, 15N, and 14N NMR spectra Научная публикация

Журнал

Russian Chemical Bulletin
ISSN: 1573-9171 , E-ISSN: 1066-5285

Вых. Данные

Год: 1993, Том: 42, Номер: 9, Страницы: 1555-1558 Страниц : 4 DOI: 10.1007/bf00699194

Авторы

Ugrak B.I. ¹ , Bogdanov V.S. ¹ , Shevelev S.A. ¹ , Dalinger I.L. ¹

Организации

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 117913, Moscow, Russian Federation

The NMR spectra (13C,15N, and14N) of N-nitropyrazoles containing nitro, methyl, and cyano groups in the pyrazole ring were investigated.13C NMR spectra were recorded under conditions of triple selective heteronuclear resonance13C-{1H,14N}. The effect of substituents in the pyrazole ring on the chemical shifts in the13C and15N NMR spectra is discussed. Coupling constants and obtained by the polarization transfer method [1H]→13C and [1H]→15N (INEPT, SPT) were measured and completely assigned.

Ugrak B.I. , Bogdanov V.S. , Shevelev S.A. , Dalinger I.L.
Nitropyrazoles. 6. Structure of N-nitropyrazoles and their 13C, 15N, and 14N NMR spectra
Russian Chemical Bulletin. 1993. V.42. N9. P.1555-1558. DOI: 10.1007/bf00699194 WOS Scopus OpenAlex

≡ Web of science:	WOS:A1993NV62800023
≡ Scopus:	2-s2.0-21344496540
≡ OpenAlex:	W2317255833