Alkylation of salts of N-(β-hydroxyalkyl)-N′-hydroxydiazeneN-oxides with alkyl halides and dimethyl sulfate

Alkylation of salts of N-(β-hydroxyalkyl)-N′-hydroxydiazeneN-oxides with alkyl halides and dimethyl sulfate Научная публикация

Журнал

Russian Chemical Bulletin
ISSN: 1573-9171 , E-ISSN: 1066-5285

Вых. Данные

Год: 1998, Том: 47, Номер: 10, Страницы: 1940-1946 Страниц : 7 DOI: 10.1007/bf02494502

Авторы

Luk'yanov O.A. ¹ , Smirnov G.A. ¹ , Nikitin S.V. ¹

Организации

1	N. D. Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, Moscow, Russian Federation

Salts of N-(β-hydroxyalkyl)-N′-hydroxydiazeneN-oxides, RCH(OH)CH2N(O)=NO− M+ (R=Me, Pri, or But; and M=Li, Na, K, Ag, NH4, or Me4N), were prepared. Their alkylation with alkyl halides R′X (X=Cl, Br, or I) and dimethyl sulfate was studied. Generally, alkylation afforded mixtures of N-(β-hydroxyalkyl)-N′-alkoxydiazeneN-oxides RCH(OH)CH2N(O)=NOR′ andO-alkyl-N-(β-hydroxyalkyl)-N-nitrosohydroxylamines RCH(OH)CH2N(NO)OR′.

Luk'yanov O.A. , Smirnov G.A. , Nikitin S.V.
Alkylation of salts of N-(β-hydroxyalkyl)-N′-hydroxydiazeneN-oxides with alkyl halides and dimethyl sulfate
Russian Chemical Bulletin. 1998. V.47. N10. P.1940-1946. DOI: 10.1007/bf02494502 WOS Scopus OpenAlex

≡ Web of science:	WOS:000077984800021
≡ Scopus:	2-s2.0-0345910741
≡ OpenAlex:	W2008308896