Synthesis of spin-labeled bispidines

Synthesis of spin-labeled bispidines Full article

Journal

Russian Chemical Bulletin
ISSN: 1573-9171 , E-ISSN: 1066-5285

Output data

Year: 2024, Volume: 73, Number: 5, Pages: 1253-1260 Pages count : 8 DOI: 10.1007/s11172-024-4241-7

Authors

Zakirov A.M. ¹ , Medved’ko A.V. ¹ , Troshin I.I. ¹ , Tretyakov E.V. ¹ , Vatsadze S.Z. ¹

Affiliations

1	N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991, Moscow, Russian Federation

Conjugates of bispidines and free radicals of the (2,2,6,6-tetramethylpiperidin-1-yl)-oxyl type were synthesized for the first time. The conjugates were obtained by the alkylation reaction of NH-bispidines with electrophilic chloro derivatives containing a free radical. The structure of the latter was established by X-ray diffraction analysis. The products obtained were characterized by IR spectroscopy, ESR spectroscopy, and high-resolution mass spectrometry.

Zakirov A.M. , Medved’ko A.V. , Troshin I.I. , Tretyakov E.V. , Vatsadze S.Z.
Synthesis of spin-labeled bispidines
Russian Chemical Bulletin. 2024. V.73. N5. P.1253-1260. DOI: 10.1007/s11172-024-4241-7 Scopus OpenAlex

Scopus:	2-s2.0-85196619436
OpenAlex:	W4399899499

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