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5,5′-(Piperazine-1,4-diyl)bis(4-chloro-3H-1,2-dithiol-3-one) Научная публикация

Журнал Molbank
ISSN: 1422-8599
Вых. Данные Год: 2022, Том: 2022, Номер: 3, Номер статьи : M1411, Страниц : DOI: 10.3390/m1411
Авторы Ogurtsov Vladimir A. 1 , Rakitin Oleg A. 1
Организации
1 N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky Prospekt, 119991 Moscow, Russia

Реферат: Conjugates of 3H-1,2-dithiol-3-ones with various biologically active compounds are intensively investigated. Although many derivatives of this class have been described in the literature, the compounds containing two dithiole cycles have been explored much less. In this communication, it was shown that the reaction of 4,5-dichloro-3H-1,2-dithiol-3-one with piperazine can selectively lead to the mono-product, 4-chloro-5-piperazin-1-yl-3H-1,2-dithiol-3-one and bis-product, 5,5′-(piperazine-1,4-diyl)bis(4-chloro-3H-1,2-dithiol-3-one). The structure of the synthesized compounds was established by elemental analysis, high resolution mass-spectrometry, 1H, 13C NMR and IR spectroscopy, and mass-spectrometry.
Библиографическая ссылка: Ogurtsov V.A. , Rakitin O.A.
5,5′-(Piperazine-1,4-diyl)bis(4-chloro-3H-1,2-dithiol-3-one)
Molbank. 2022. V.2022. N3. M1411 . DOI: 10.3390/m1411 WOS Scopus OpenAlex
Идентификаторы БД:
Web of science: WOS:000856867100001
Scopus: 2-s2.0-85138660948
OpenAlex: W4286610833
Цитирование в БД:
БД Цитирований
OpenAlex 1
Scopus 1
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