Unexpected Formation of Thioglycolurils Precursors | Sciact - научная деятельность

Unexpected Formation of Thioglycolurils Precursors Научная публикация

Журнал

Journal of Heterocyclic Chemistry
ISSN: 0022-152X , E-ISSN: 1943-5193

Вых. Данные

Год: 2014, Том: 52, Номер: 6, Страницы: 1858-1863 Страниц : 6 DOI: 10.1002/jhet.2305

Авторы

Gazieva Galina A. ¹ , Kravchenko Angelina N. ¹

Организации

1	N.D. Zelinsky Institute of Organic Chemistry; Russian Academy of Sciences; Moscow 119991 Russia

Unexpectedly, nitrosation of 5,7-dialkyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazine-6-ones(thiones) with sodium nitrite in glacial AcOH led to 3,3′-bis(5,7-dialkyl-1-nitroso-6-oxo(thioxo)-1,4,4a,5,7,7a-hexahydroimidazo[4,5-e]-1,2,4-triazinyl)disulfides that decomposed spontaneously into 1,3-dialkyl-5-thioxohexahydroimidazo[4,5-d]imidazol-2(1H)-ones(thiones) in DMSO-d6 in the presence of water.

Gazieva G.A. , Kravchenko A.N.
Unexpected Formation of Thioglycolurils Precursors
Journal of Heterocyclic Chemistry. 2014. V.52. N6. P.1858-1863. DOI: 10.1002/jhet.2305 WOS Scopus OpenAlex

≡ Web of science:	WOS:000363901300039
≡ Scopus:	2-s2.0-84946481851
≡ OpenAlex:	W2358083529