Unexpected Formation of Thioglycolurils Precursors Full article
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Journal of Heterocyclic Chemistry
ISSN: 0022-152X , E-ISSN: 1943-5193 |
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| Output data | Year: 2014, Volume: 52, Number: 6, Pages: 1858-1863 Pages count : 6 DOI: 10.1002/jhet.2305 | ||
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Abstract:
Unexpectedly, nitrosation of 5,7-dialkyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazine-6-ones(thiones) with sodium nitrite in glacial AcOH led to 3,3′-bis(5,7-dialkyl-1-nitroso-6-oxo(thioxo)-1,4,4a,5,7,7a-hexahydroimidazo[4,5-e]-1,2,4-triazinyl)disulfides that decomposed spontaneously into 1,3-dialkyl-5-thioxohexahydroimidazo[4,5-d]imidazol-2(1H)-ones(thiones) in DMSO-d6 in the presence of water.
Cite:
Gazieva G.A.
, Kravchenko A.N.
Unexpected Formation of Thioglycolurils Precursors
Journal of Heterocyclic Chemistry. 2014. V.52. N6. P.1858-1863. DOI: 10.1002/jhet.2305 WOS Scopus OpenAlex
Unexpected Formation of Thioglycolurils Precursors
Journal of Heterocyclic Chemistry. 2014. V.52. N6. P.1858-1863. DOI: 10.1002/jhet.2305 WOS Scopus OpenAlex
Identifiers:
| ≡ Web of science: | WOS:000363901300039 |
| ≡ Scopus: | 2-s2.0-84946481851 |
| ≡ OpenAlex: | W2358083529 |