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Convenient Synthesis of Geminal Bishydroperoxides by the Reaction of Ketones with Hydrogen Peroxide Научная публикация

Журнал Synthetic Communications
ISSN: 1532-2432 , E-ISSN: 0039-7911
Вых. Данные Год: 2007, Том: 37, Номер: 8, Страницы: 1281-1287 Страниц : 7 DOI: 10.1080/00397910701226384
Авторы Terent'ev A.O. 1 , Platonov M.M. 1 , Ogibin Y.N. 1 , Nikishin G.I. 1
Организации
1 N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences , Moscow, Russia

Реферат: A convenient procedure was developed for the synthesis of geminal bishydroperoxides by the sulfuric acid–catalyzed reaction of ketones with hydrogen peroxide in THF. Gem‐bishydroperoxides were prepared by the reactions of five‐ to seven‐membered cycloalkanones without additional purification in 80–95% yields with a purity of more than 95%; their acyclic analogs were prepared in 43–72% yields.
Библиографическая ссылка: Terent'ev A.O. , Platonov M.M. , Ogibin Y.N. , Nikishin G.I.
Convenient Synthesis of Geminal Bishydroperoxides by the Reaction of Ketones with Hydrogen Peroxide
Synthetic Communications. 2007. V.37. N8. P.1281-1287. DOI: 10.1080/00397910701226384 WOS Scopus OpenAlex
Идентификаторы БД:
≡ Web of science: WOS:000247620500026
≡ Scopus: 2-s2.0-34247099810
≡ OpenAlex: W1963741535
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