Convenient Synthesis of Geminal Bishydroperoxides by the Reaction of Ketones with Hydrogen Peroxide Full article
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Synthetic Communications
ISSN: 1532-2432 , E-ISSN: 0039-7911 |
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| Output data | Year: 2007, Volume: 37, Number: 8, Pages: 1281-1287 Pages count : 7 DOI: 10.1080/00397910701226384 | ||
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Abstract:
A convenient procedure was developed for the synthesis of geminal bishydroperoxides by the sulfuric acid–catalyzed reaction of ketones with hydrogen peroxide in THF. Gem‐bishydroperoxides were prepared by the reactions of five‐ to seven‐membered cycloalkanones without additional purification in 80–95% yields with a purity of more than 95%; their acyclic analogs were prepared in 43–72% yields.
Cite:
Terent'ev A.O.
, Platonov M.M.
, Ogibin Y.N.
, Nikishin G.I.
Convenient Synthesis of Geminal Bishydroperoxides by the Reaction of Ketones with Hydrogen Peroxide
Synthetic Communications. 2007. V.37. N8. P.1281-1287. DOI: 10.1080/00397910701226384 Scopus OpenAlex
Convenient Synthesis of Geminal Bishydroperoxides by the Reaction of Ketones with Hydrogen Peroxide
Synthetic Communications. 2007. V.37. N8. P.1281-1287. DOI: 10.1080/00397910701226384 Scopus OpenAlex
Identifiers:
| Scopus: | 2-s2.0-34247099810 |
| OpenAlex: | W1963741535 |